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1 Foster, I and Kesselman, C (eds) (1999) The Grid: Blueprint for a New Computing Infrastructure San Francisco, CA: Morgan Kaufmann Publishers 2 Hillmann D (2001) Using Dublin core, Dublin Core Metadata Initiative, dublincoreorg/documents/usageguide 3 Lassila, O and Swick, R (1999) Resource Description Framework (RDF) Model and Syntax Speci cation, W3C, wwww3corgREC-rdf-syntax-19990222 4 Berners-Lee, T, Hendler, J and Lassila, O (2001) The semantic web Scienti c American, May, 34 43 5 Pearson, D (2002) Data Requirements for the Grid: Scoping Study Report UK Grid Database Taskforce 6 Global Grid Forum, Global Grid Forum Security Working Group, wwwgridforumorg, 2002 7 Global Grid Forum, Accounting Models Research Group, wwwgridforumorg, 2002 8 Tierney, B, Aydt, R, Gunter, D, Smith, W, Taylor, V, Wolski, R and Swany, M (2002) A Grid Monitoring Architecture, Global Grid Forum, GWD-Perf-16-2 9.

Vusse (1966), in which mixing was shown to affect the distribution of chlorinated products. The chlorination of acetone is also a mixing-sensitive gas liquid reaction as described in Example 13-6. Example 13-6: Chlorination of Acetone: Mixing-Sensitive Gas Liquid Reaction (Paul et al., 1981) Goal: determination of the cause of reduced selectivity in a manufacturing scale gas liquid competitive-consecutive reaction and modi cation of the reactor to achieve target selectivity Issue: decrease in selectivity experienced on scale-up This example presents reactor design problems experienced in the scale-up of a classical competitive-consecutive reaction from bench to manufacturing scale. Expected selectivity was not achieved initially, and a revised reactor was required. The chlorination of acetone is a very fast reaction that produces both monochloroacetone and dichloroacetones as well as polychlorinated species. The product desired is monochloroacetone. The reactions are shown in Figure 13-16 and the product distribution in Figure 13-17. Elevated local concentrations will increase the local reaction rates. As is often the case, the di- and polychlorinated species not only reduce yield but cause ongoing yield and purity problems in subsequent steps of a multistep synthesis because of their reactivity. The rate constant ratio between mono- and dichlorinated species is very unfavorable for making high-purity monochlorinated species, thereby requiring excellent mixing, a very high molar ratio of acetone to chlorine (>10 : 1), and subsequent acetone recovery. Laboratory results: Semibatch addition of chlorine gas to liquid acetone in a 5 L ask; 98% monochloro, 2% overchlorinated products.

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Global Grid Forum, Scheduling and Resource Management Area, wwwgridforumorg, 2002 10 Graefe, G (1990) Encapsulation of parallelism in the volcano query processing system, SIGMOD Conference Atlantic City, NJ: ACM Press 11 Smith, J, Sampaio, S D F M, Watson, P and Paton, N W (2000) Polar: An architecture for a parallel ODMG compliant object database, ACM CIKM International Conference on Information and Knowledge Management McLean, VA: ACM Press 12 Smith, J, Gounaris, A, Watson, P, Paton, N W, Fernandes, A A A and Sakellariou, R (2002) Distributed query processing on the grid Proceedings of the 3rd International Workshop on Grid Computing (GRID 2002), in LNCS 2536, Springer-Verlag, pp 279 290 13 Cattell, R (1997) Object Database Standard: ODMG 20 San Francisco, CA: Morgan Kaufmann Publishers 14 Smith, J, Watson, P, Sampaio, S D F M and Paton, N W.

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(2002) Speeding up navigational requests in a parallel object database system EuroPar 2002 , LNCS 2400, Paderborn, Germany, pp 332 341, 2002 15 Shiers, J (1998) Building a multi-petabyte database: The RD45 project at CERN, in Loomis, M E S and Chaudhri, A B (eds) Object Databases in Practice New York: Prentice Hall, pp 164 176 16 De Roure, D, Jennings, N and Shadbolt, N (2001) Research Agenda for the Semantic Grid: A Future e-Science Infrastructure UKeS-2002-02, Edinburgh, UK: UK National e-Science Centre 17 Sheth, A P and Larson, J A (1990) Federated database systems for managing distributed, heterogeneous and autonomous databases ACM Computing Surveys, 22(3), 183 236 18 Lahiri, T, Abiteboul, S and Widom, J (1999) Ozone: Integrating structured and semistructured data, Seventh Intl Workshop on Database Programming Languages Scotland: Kinloch Rannoch 1999..

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